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Ah yeah, I didn't calculate why I necessary 5M of NaOH. I just made use of that amount to ensure full neutralisation. A tad overkill. Even though this method operates and gives a lot of spice, it's very wasteful of NaOH.
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EDIT: I did the titration. I applied 500ml of my inventory solution HCl, and titrated against my inventory solution of NaOH. HCl is 0.001M and NaOH is 5M.
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